Trace Environmental Quantitative Analysis

Including Student-Tested Experiments

Gebonden Engels 2020 3e druk 9780367445331
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Samenvatting

A thorough and timely update, this new edition presents principles, techniques, and applications in this sub-discipline of analytical chemistry for quantifying traces of potentially toxic organic and inorganic chemical substances found in air, soil, fish, and water, as well as serum, plasma, urine, and other body fluids. The author addresses regulatory aspects, calibration, verification, and the statistical treatment of analytical data including instrument detection limits; quality assurance/quality control; sampling and sample preparation; and techniques that are used to quantify trace concentrations of organic and inorganic chemical substances.

Key Features:

Fundamental principles are introduced for the more significant experimental approaches to sample preparation

Principles of instrumental analysis (determinative techniques) for trace organics and trace inorganics analysis

An introduction to the statistical treatment of trace analytical data

How to calculate instrument detection limits based on weighted least squares confidence band calibration statistics

Includes an updated series of student-tested experiments

Specificaties

ISBN13:9780367445331
Taal:Engels
Bindwijze:Gebonden
Aantal pagina's:738
Uitgever:Taylor & Francis Ltd
Druk:3

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Inhoudsopgave

Preface to the Third Edition. About the Author. About the Contributors. Chapter 1 Introduction to Trace Environmental Quantitative Analysis (TEQA). Chapter 2 Calibration, Verification, Quantification, Statistical Treatment of Analytical Data, Detection Limits, and Quality Assurance/ Quality Control. Chapter 3 Sample Preparation Techniques to Isolate and Recover Organics and Inorganics. Chapter 4 Determinative Techniques to Measure Organics and Inorganics. Chapter 5 Student- Tested Laboratory Experiments. Appendix A: Glossary. Appendix B: QA/ QC Illustrated. Appendix C: A Primer on the Basics of Probability and Statistics for Some and a Quick Review for Others. Appendix D: Quality Control for Environmental- Health TEQA: Levey– Jennings Plots and Westgard Rules. Appendix E: Innovative Sample Prep Flow Charts for TEQA. Appendix F: Quantitating VOCs in Serum Using Automated Headspace-SPME/ Cryo- Focusing/ Isotope Dilution/ Capillary GC-MS. Appendix G: Using a Pooled Standard Deviation to Find the Uncertainty in the Percent Recovery for the Priority Pollutant Phenol Using Reversed- Phase SPE from Spiked Water by Converting Phenol to its Pyrazol- 3- One Complex: Comparing In Situ vs. Synthesized Experimental Approaches. Appendix H: Laboratory Glass & Instrument Designs. Appendix I: Useful Potpourri for Environmental Analytical Chemists. Appendix J: Contributing Authors: Brief Introduction. Index.

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